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Service

  • Thermochemical, thermokinetic, thermogravimetric and calorimetric analyses in the temperature range from 10 °C to 800 °C, also at pressures up to 400 bar, bianca [dot] stoerr [at] chemie [dot] tu-freiberg [dot] de (Dipl.- Nat.Nat. Störr), Andreas [dot] Lissner [at] chemie [dot] tu-freiberg [dot] de (Dr. Lißner), Dr. Seidel
  • Calorimetric analyses near room temperature on extremely small sample quantities (mg range), also for the detection of pollutants and for odour analyses, Johannes [dot] Lerchner [at] chemie [dot] tu-freiberg [dot] de (Dr. Lerchner)
  • Thermochemical calculations, also for the optimisation of data sets and process parameters, Klaus [dot] Bohmhammel [at] chemie [dot] tu-freiberg [dot] de (Prof. Bohmhammel)
  • Topographic investigation using atomic force microscopes (AFM NX10) , Andreas [dot] Lissner [at] chemie [dot] tu-freiberg [dot] de (Dr. Lißner)

Technical equipment of the Institute of Physical Chemistry

The list of technical equipment and methods is intended to illustrate the possibilities of working on, in and with the IPC.

Spectroscopic methods

  • X-ray photoelectron spectroscopy (XPS) and UPS, TDS, Andreas Lißner, Zi. 213, Form for the order of an XPS measurement
  • UV/Vis (solution)
  • IR (DRIFT, KBr, gas analysis), Zi. 218
  • X-ray powder diffractometer D2 Phaser (Bruker), Zi. 213

Thermal methods

  • C80 (Setaram), Zi. 221
  • TG-DSC, Zi.221
  • TG-DSC with MS and IR, Zi. 218

Adsorption measurements

  • BET nitrogen cryoadsorption using Sievert's apparatus, Zi. 213
  • BET nitrogen cryoadsorption BELSORP-mini II, contact: Regina Hüttl
  • High-pressure adsorption measurements with hydrogen, nitrogen and carbon dioxide, Zi. 213

Chromatographic methods

  • Gas chromatographs from HP and Agilent with FID, WLD, Zi. 220
  • HPLC (Knauer), column oven, UV/Vis and refractive index, Zi. 218

Small equipment

  • Quartz microbalance
  • Steriliser CertoClav, steam up to 140°C/approx. 2.7bar, max. 5x 1L bottles, room 220

Experimental techniques

  • Swivel and autoclave technique, rooms 217, 222 and overnight lab 2.105
  • Glove box for solids (room 220) and for liquids (room 217)

Internal

  • Chemicals database of Physical Chemistry: Database